Production Process of Glacial Acetic Acid
The production process of glacial acetic acid can be divided into the following steps:
Raw Material Preparation: The main raw materials for glacial acetic acid are ethanol and an oxidizing agent. Ethanol is typically obtained through fermentation or chemi...
[Leakage Disposal]: Evacuate personnel in the contaminated area of glacial acetic acid leakage to a safe area, prohibit irrelevant personnel from entering the contaminated area, and cut off the source of fire. It is recommended that emergency handling personnel wear self-contained breathing appar...
[Storage and Transportation Precautions]: Glacial acetic acid should be stored in a cool and well-ventilated warehouse. Keep it away from kindling and heat sources. The warehouse temperature should not exceed 30℃. In winter, anti-freezing measures should be taken to prevent freezing. Maintain the...
Pure anhydrous acetic acid (glacial acetic acid) is a colorless, hygroscopic liquid with a freezing point of 16.6°C (62°F). Upon solidification, it forms colorless crystals. Although it is classified as a weak acid based on its dissociation ability in aqueous solutions, acetic acid is corrosive, ...
When water is added to acetic acid, the total volume of the mixture decreases, and the density increases until the molecular ratio reaches 1:1, corresponding to the formation of orthoacetic acid (CH₃C(OH)₃), a monobasic acid. Further dilution does not result in additional volume changes.
Molecul...
Acetic acid is a colorless liquid with a strong, pungent odor. It has a melting point of 16.6°C, a boiling point of 117.9°C, and a relative density of 1.0492 (20/4°C), making it denser than water. Its refractive index is 1.3716. Pure acetic acid solidifies into an ice-like solid below 16.6°C, whi...
Acetic acid is a saturated carboxylic acid containing two carbon atoms and is an important oxygen-containing derivative of hydrocarbons. Its molecular formula is C₂H₄O₂, with the structural formula CH₃COOH, and its functional group is the carboxyl group. As the main component of vinegar, glacial ...
The above three processes are commonly used in formic acid production. As an important organic chemical raw material, formic acid is widely applied in industries such as textiles, leather, and rubber. Therefore, advancements and optimization in production technology are crucial for improving effi...
Formic Acid Gas-Phase Method
The gas-phase method is a relatively newer approach for formic acid production. The process flow is as follows:
(1) Raw Material Preparation:
Methanol and air are prepared, with methanol undergoing purification and dehydration.
(2) Gas-Phase Oxidation Reaction:
Pr...
Carbon Monoxide-Water Reduction Method
This is another method for producing formic acid. The process flow is as follows:
(1) Raw Material Preparation:
Carbon monoxide and water are pretreated to achieve the required purity and concentration.
(2) Reduction Reaction:
Carbon monoxide and water are h...
Production Processes of Formic Acid
Formic acid is an organic compound with the chemical formula HCOOH. It can be produced through various methods, including methanol oxidation, carbon monoxide-water reduction, and gas-phase processes.
Methanol Oxidation Method
The methanol oxidation method is o...
Determination of Formic Acid
1. Scope
Applicable to the determination of industrial-grade formic acid.
2. Test Method
2.1 Determination of Formic Acid Content
2.1.1 Principle
Formic acid is a weak acid and can be titrated with a standard NaOH solution using phenolphthalein as the indicator. The r...